Carbon 13 Nuclear Magnetic Resonance Spectroscopy of Myoglobins and Ribonuclease A Carboxymethylated with Enriched [2-13C]Bromoacetate
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منابع مشابه
Carbon-13 nuclear magnetic resonance spectroscopy.
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High-resolution Fourier transform nuclear magnetic resonance was used to observe the natural abundance (13)C spectrum of a 0.02 M solution of bovine pancreatic ribonuclease A. Peaks assignable to only three carbons were easily observed after 10 hr of signal averaging. A number of tentative assignments were made. As expected, the (13)C spectrum was appreciably richer in detail than the correspon...
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The 13C n.m.r. spectrum of Forssman hapten was obtained at 25.16 MHz in [3H] chloroform/[2H] methanol (1:1, v/v), using purified glycosphinogolipid from canine intestinal mucosa (glycolipid I). All amide, olefin, anomeric, intersaccharide glycosidic ether, amide linkage, methyl and many methylene resonances were resolved and assigned. Analysis of the anomeric region reveals the following pentag...
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C-13 ~7~JL-l,t':*JL-J... 7N:Fc I-" ~m~)-c;(" ~ :..~.:L I) 70)~""J...7 Nj'C I-" Io:.t:fl'*' t!."ft.:J5I:t'Q~.~&:fit;~.HL-t;:o DM50-d. ..~*~TQ ~ I'C-NMR A~? .. ""0) ft~ $-' 7 I~f~_.t.: $-' 7 IT Q .: ~ ~ft}rJ. 1fI.0)1r.~$-' 7 I~1nE tt;:o ;(" ~ :..0);( -1tl -"".I~.:L~ 70).-87 ~ /.to)~~t.:~ Q;( -1-v:..-M~~~l,~T <. ;(" ~ /O)~ ;(-1-V:"-Z-7NM~~t.:~Qea.~t.:~TQo I-~;(-1-D-"";(7~:"-~~;(-1-D-N .:L ~ 70)~~~...
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ژورنال
عنوان ژورنال: Journal of Biological Chemistry
سال: 1972
ISSN: 0021-9258
DOI: 10.1016/s0021-9258(19)45145-4